HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl methyl(piperidin-4-yl)carbamate hydrochloride → Benzyl 1-[4-(3-cyclohexyl-1-methyl-4-oxo-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-6-yl)-3-ethoxyphenyl]-4-piperidinyl(methyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl methyl(piperidin-4-yl)carbamate hydrochloride | HCID 18677745 | — |
| Reactant | HCID 136005963 | HCID 136005963 | — |
| Product | Benzyl 1-[4-(3-cyclohexyl-1-methyl-4-oxo-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-6-yl)-3-ethoxyphenyl]-4-piperidinyl(methyl)carbamate | HCID 136333210 | 77% |
Reaction Steps
The same reaction procedure as in Example 27 was performed, except that the compound obtained in Example 85 was used in place of the compound obtained in Example 26, and benzyl methyl(4-piperidinyl)carbamate hydrochloride was used in place of N-methylpiperazine. In this manner, 234 mg (77%) of the captioned compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268128B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-0bfbadf1fe8b467f8152c5da47e8a2a7 |
| Source note | uspto-grants-2007_09 |