HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178479266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178453980 | HCID 178453980 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178479266 | HCID 178479266 | — |
Reaction Steps
{cis-4-[4-(Pyrrolidine-1-carbonyl)-[1,2,3]triazol-1-yl]-cyclohexyl}-carbamic acid tert-butyl ester (406 mg) was stirred 1 h in a mixture of 4.6 M HCl in EtOAc (3.6 ml) and MeOH (0.84 ml). The solvent was evaporated to yield the product (335 mg, quant.) as white foam after drying on the high vacuum. MS 264.3 (100, [M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268154B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-2d7b70450baf45e48253b642f2ad70b2 |
| Source note | uspto-grants-2007_09 |