HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178498823, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178498825 | HCID 178498825 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178498823 | HCID 178498823 | — |
Reaction Steps
A solution of 1-(cis-4-tert-butoxycarbonylamino-cyclohexyl)-1H-[1,2,3]triazole-4-carboxylic acid methyl ester (2.53 g) in a mixture of 4.6 M HCl in EtOAc (25 ml) and MeOH (7.6 ml) was stirred 1 h at RT. The product precipitated and was collected by filtration. Yield: 1.36 g (58%). White powder. MS 225.0 (100, [M+H]+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268154B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-354654a701034fbf8ff94ec03c79af3f |
| Source note | uspto-grants-2007_09 |