huagongshe.com
HRID916052

反应详情

EQUATION

反应方程式

HRID 916052 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：COC(=O)c1cn([C@H]2CC[C@@H](NC(=O)OC(C)(C)C)CC2)nn1
HCID178498825

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cn([C@H]2CC[C@@H](N)CC2)nn1.Cl.Cl
HCID178498823

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CO
溶剂HCID887

Methanol

CH4O

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

A solution of 1-(cis-4-tert-butoxycarbonylamino-cyclohexyl)-1H-[1,2,3]triazole-4-carboxylic acid methyl ester (2.53 g) in a mixture of 4.6 M HCl in EtOAc (25 ml) and MeOH (7.6 ml) was stirred 1 h at RT. The product precipitated and was collected by filtration. Yield: 1.36 g (58%). White powder. MS 225.0 (100, [M+H]+).

WORKUP

后处理

  1. customThe product precipitated
  2. filtrationwas collected by filtration