HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 1-Benzyl-3-aminopyrrolidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 10236311 | HCID 10236311 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-Benzyl-3-aminopyrrolidine | HCID 2756613 | — |
Reaction Steps
The 1-benzyl-3-aminopyrrolidine monomethanesulfonate (2 g) was dissolved in water (5 mL). And then 30% sodium hydroxide was added to the solution to isolate 1-benzyl-3-aminopyrrolidine. The solution was extracted with toluene (20 mL) and then concentrated. Thus, oily 1-benzyl-3-aminopyrrolidine (1.10 g) was recovered.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268236B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-9b8db400522744ae8a77d05caa394ff2 |
| Source note | uspto-grants-2007_09 |