HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethyl-3-pyrroline → 4-(2,5-dimethyl-2,5-dihydropyrrol-1-yl)naphthalene-1-carbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethyl-3-pyrroline | HCID 101066 | — |
| Reactant | 1-Cyano-4-fluoronaphthalene | HCID 2736734 | — |
| Product | 4-(2,5-dimethyl-2,5-dihydropyrrol-1-yl)naphthalene-1-carbonitrile | HCID 11708585 | 3.4% |
Reaction Steps
The title compound (1 mg, 3% yield) was prepared as described for 196MBT2-4 from 1-cyano-4-fluoronaphthalene (20 mg, 0.117 mmol) and 2,5-dimethyl-2,5-dihydro-1H-pyrrole (45 mg, 0.468 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268232B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-91daea77a886464a8eede0658247147b |
| Source note | uspto-grants-2007_09 |