HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → HCID 69385416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 68981033 | HCID 68981033 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69385416 | HCID 69385416 | — |
Reaction Steps
A solution of 3-(4-hydroxybutyl)phenyl acetate (416 mg) in DCM (10 mL) was treated with carbon tetrabromide (1.16 g) and triphenylphosphine (791 mg) and stirred at room temperature for 15 min prior to concentration in vacuo. The residue was purified by chromatography (SPE, DCM-petrol 1:1) to give the title compound. LCMS RT=3.58 min
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07271197B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-5c0f3dec3e8b4df8aff65ef2f6eb4085 |
| Source note | uspto-grants-2007_09 |