HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acryloyl chloride → HCID 23070525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | 2-Dimethylaminopyridine | HCID 21885 | — |
| Reactant | HCID 23070529 | HCID 23070529 | — |
| Product | HCID 23070525 | HCID 23070525 | — |
Reaction Steps
An excess of 2-(phenylthio)ethanethiol is reacted with epichlorohydrin to form 1,3-bis(2-(phenylthio)ethylthio)propan-2-ol. In the final step, the 1,3-bis(2-(phenylthio)ethylthio)propan-2-ol is reacted with a acryloyl chloride in the presence of a tertiary alkyl amine and dimethylaminopyridine to form 1,3-bis(2-(phenylthio)ethylthio)propan-2-yl acrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07271283B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-8a9b1a6b99094c2db7413ed89cdbe436 |
| Source note | uspto-grants-2007_09 |