Dichloromethane → HCID 87824249, compound

Participants

Reaction Steps

To a dried round bottom flask was added methylene chloride (2 mL), the product of Example 86 (0.110 g; 0.217 mmol), oxalyl chloride (0.02 mL, 0.217 mmol), and DMF (1 drop; cat.). The reaction mixture was stirred for 1.5 hours at room temperature. Toluene (1 mL) was added to the reaction mixture and the volatiles were removed in vacuo.

Provenance & Evidence