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HRID917241

反应详情

EQUATION

反应方程式

HRID 917241 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

2 次

结构：CCCCCCCCC1(CCCCCCCC)c2ccccc2-c2ccc(C(=O)O)cc21
HCID21982080

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCC1(CCCCCCCC)c2ccccc2-c2ccc(C(=O)Cl)cc21
HCID21982108

未命名化合物

PROCEDURE

实验过程

9,9-Dioctyl-9H-fluorene-2-carboxylic acid (32.36 g, 74.5 mmole) was refluxed in thionyl chloride (93 g, 782 mmole) for 8 hrs. Unreacted thionyl chloride was distilled off and the residue material used without further purification.

WORKUP

后处理

  1. distillationwas distilled off
  2. customthe residue material used without further purification