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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 917241Generated: October 26, 2026

Thionyl Chloride → HCID 21982108, compound

https://huagongshe.com/reaction/917241

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
Reactant9,9-Dioctyl-9H-fluorene-2-carboxylic AcidHCID 21982080—
ProductHCID 21982108HCID 21982108—

Reaction Steps

9,9-Dioctyl-9H-fluorene-2-carboxylic acid (32.36 g, 74.5 mmole) was refluxed in thionyl chloride (93 g, 782 mmole) for 8 hrs. Unreacted thionyl chloride was distilled off and the residue material used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07271406B2
Source datasetuspto-grants-2007_09
ORD IDord-9cfe1f9b4a994e3588cba9faa70f8751
Source noteuspto-grants-2007_09