HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Disulfide → HCID 178440705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | 3-tert-Butylaniline | HCID 79334 | — |
| Reactant | Sulfur | HCID 5362487 | — |
| Product | HCID 178440705 | HCID 178440705 | 88.3% |
Reaction Steps
In a autoclave of 3 liters, 1341g of meta-tert-butylaniline, 820g of carbon disulfide and 288g of sulfur were placed, the reaction was carried out under the same conditions as above. After cooling, 1765g of 5-tert-butyl-(2-mercapto)benzothiazole was obtained. (yield: 88.3%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03967951 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-421e4a41fbbd453a833ef8d9bcd4a658 |
| Source note | uspto-grants-1976_07 |