Carbon Disulfide → HCID 178440705, compound

HRID 917804Notes

Reaction equation

HRID 917804 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:9]=[CH:10][CH:11]=1)[NH2:8])([CH3:4])([CH3:3])[CH3:2].[S].[C:13](=[S:15])=[S:14]>>[C:1]([C:5]1[CH:11]=[CH:10][C:9]2[S:14][C:13]([SH:15])=[N:8][C:7]=2[CH:6]=1)([CH3:4])([CH3:2])[CH3:3]

Participants

4

Reactant 3

HCID 6348Carbon DisulfideHCID 793343-tert-ButylanilineHCID 5362487Sulfur

Product 1

HCID 178440705HCID 178440705, compoundYield 88.3%

Procedure

In a autoclave of 3 liters, 1341g of meta-tert-butylaniline, 820g of carbon disulfide and 288g of sulfur were placed, the reaction was carried out under the same conditions as above. After cooling, 1765g of 5-tert-butyl-(2-mercapto)benzothiazole was obtained. (yield: 88.3%)

Workup

  1. temperatureAfter cooling

Sources & evidence

ORD record
ord-421e4a41fbbd453a833ef8d9bcd4a658
Source dataset
uspto-grants-1976_07
Patent number
US03967951

Reaction notes

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