HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylaminoethyl chloride → HCID 68129628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylaminoethyl chloride | HCID 13364 | — |
| Reactant | HCID 68129192 | HCID 68129192 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68129628 | HCID 68129628 | — |
Reaction Steps
Thirty grams of 2,6-dimethyl-4-(3-amino-6-chlorophenyl)-1,4-dihydropyridine-3,5-dicarboxylic acid diethyl ester (melting point 210°) and 15 ml of 2-diethylaminoethyl chloride are heated for 15 minutes to about 200° and the mixture is taken up in hot water, rendered alkaline after addition of ice and extracted with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03968117 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-84a6bc845a114e5381dfd17383be66f0 |
| Source note | uspto-grants-1976_07 |