HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 86733670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Hydrogen iodide | HCID 24841 | — |
| Reactant | HCID 86733671 | HCID 86733671 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86733670 | HCID 86733670 | — |
Reaction Steps
N-p-iodobenzyl-N',N"-dimethylguanidine sulphate was dissolved in water, strongly basified with sodium hydroxide, and the base extracted with ether. The ether, on evaporation, gave an oil which was dissolved in water, neutralised with dilute hydriodic acid and evaporated, to yield N-p-iodobenzyl-N',N"-dimethylguanidine hydriodide, m.p. 235°-239°, after recrystallisation from methanol-ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03968243 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-60c640bb13904f0e82613639df3cb50f |
| Source note | uspto-grants-1976_07 |