HuagongsheHuagongshe Chemistry Print Report · For research reference only
Zincchloride → HCID 68139610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Zincchloride | HCID 3007855 | — |
| Reactant | HCID 21522704 | HCID 21522704 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68139610 | HCID 68139610 | 63% |
Reaction Steps
To a solution of 1-(3-pyridylmethyl)-3-(4-butyrylphenyl)urea (2.98 g., 0.01 mole) in 200 ml. of methanol was added a solution of anhydrous zinc chloride (0.68 g., 0.005 mole) in 50 ml. of methanol. After standing overnight the solution was concentrated in vacuo to give 2.3 g. of white solid. This was a 63% yield of 1-(3-pyridylmethyl)-3-(4-butyrylphenyl)urea zinc chloride complex.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03969357 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-224c27d5b6d349b3b7a725d64060af86 |
| Source note | uspto-grants-1976_07 |