Zincchloride → HCID 21522707, compound

Participants

Reaction Steps

To a solution of 1-(3-pyridylmethyl)-3-(4 -cyanophenyl)urea (2.52 g., 0.01 mole) in 100 ml. of methanol was added anhydrous zinc chloride (0.68 g., 0.005 mole) dissolved in 50 ml. of methanol. A solid suspension formed and after stirring 1 hr. the solid was filtered off and air dried. The product was 2.33 g. which was a 72% yield of 1-(3-pyridylmethyl)-3-(4-cyanophenyl)urea zinc chloride complex.

Provenance & Evidence