HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N,N-Diethyl-N-[(3-phenoxyphenyl)methyl]ethanaminium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Phenoxybenzyl chloride | HCID 93291 | — |
| Reactant | HCID 70567605 | HCID 70567605 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | N,N-Diethyl-N-[(3-phenoxyphenyl)methyl]ethanaminium chloride | HCID 162156 | — |
Reaction Steps
18.2 g of the chlorinated product of m-tolylphenyl ether containing 13.2 g of 3-phenoxybenzyl chloride was treated with a solution of 9.1 g of triethylamine in 60 ml of benzene in the same manner as described in Example 1. Thus, 17.8 g of colorless, needle-like 3-phenoxybenzyl triethyl ammonium chloride was obtained (hygroscopic, no clear m.p.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03969393 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-9d9658ba3bf342f2bb42b2a0c40b31c9 |
| Source note | uspto-grants-1976_07 |