huagongshe.com
HRID918203

反应详情

EQUATION

反应方程式

HRID 918203 的结构方程式

REACTANTS

反应物

2
结构：NCc1ccccc1
HCID7504

Benzylamine

C7H9N

结构：CC(C(=O)Cl)c1cc(C(C)(C)C)c(O)c(C(C)(C)C)c1
HCID19830138

未命名化合物

PRODUCTS

生成物

1
结构：CC(C(=O)NCc1ccccc1)c1cc(C(C)(C)C)c(O)c(C(C)(C)C)c1
HCID86733699

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCCC
溶剂HCID8900

Heptane

C7H16

2 次

PROCEDURE

实验过程

To a solution of 22.4 g of benzyl amine (0.21 mol) in 100 ml of heptane 29.6 g of 4-hydroxy-3,5-di-tert.-butylphenyl-propionic acid-chloride (0.1 mol) -- dissolved in 200 ml of heptane -- were added dropwise at 20°C, then the solution was boiled under reflux for 3 hours. Working up followed in the manner described in Example 12.

WORKUP

后处理

  1. additionwere added dropwise at 20°C
  2. temperatureunder reflux for 3 hours