HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 86733699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 4-Hydroxy-3,5-di-tert.-butylphenyl-propionic acid-chloride | HCID 19830138 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | HCID 86733699 | HCID 86733699 | — |
Reaction Steps
To a solution of 22.4 g of benzyl amine (0.21 mol) in 100 ml of heptane 29.6 g of 4-hydroxy-3,5-di-tert.-butylphenyl-propionic acid-chloride (0.1 mol) -- dissolved in 200 ml of heptane -- were added dropwise at 20°C, then the solution was boiled under reflux for 3 hours. Working up followed in the manner described in Example 12.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03969530 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-2524b7ffb2254c94aa27e5f042fbd9f2 |
| Source note | uspto-grants-1976_07 |