HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → N,N-diethyl 3,7,11-trimethyldodeca-2,4,10-trienylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 11-Chloro-3,7,11-trimethyldodeca-2,4-dienyl bromide | HCID 53871432 | — |
| Reactant | HCID 54370561 | HCID 54370561 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N,N-diethyl 3,7,11-trimethyldodeca-2,4,10-trienylamine | HCID 53837124 | — |
Reaction Steps
Five grams of 1 bromo-3,7,11-trimethyldodeca-2,4,10-triene in 25 ml. of benzene is mixed with 4 g. of diethylamine and the mixture stirred for about three hours. Methylene chloride (50 ml.) is added and the mixture washed with dilute sodium hydroxide and then water and evaporated to yield N,N-diethyl 3,7,11-trimethyldodeca-2,4,10-trienylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03970704 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-fd1ec86af4c24fd3b2e9cc477e948b13 |
| Source note | uspto-grants-1976_07 |