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HRID918404

反应详情

EQUATION

反应方程式

HRID 918404 的结构方程式

REACTANTS

反应物

2
结构：CCOC(C=[N+]=[N-])OCC
HCID21520892

Ethane, 2-diazo-1,1-diethoxy-

C6H12N2O2

结构：C[C@]12C=CC(=O)C=C1[C@@H](F)C[C@@H]1[C@@H]2[C@@H](O)C[C@@]2(C)[C@H]1C[C@@H](O)[C@]2(O)C(=O)CO
HCID22793229

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(CO[C@@H]1C[C@H]2[C@@H]3C[C@H](F)C4=CC(=O)C=C[C@]4(C)[C@H]3[C@@H](O)C[C@]2(C)[C@@]1(O)C(=O)CO)OCC
HCID22791783

未命名化合物

PROCEDURE

实验过程

A solution of 2,2-diethoxy-1-diazoethane (prepared from 0.18 mole of precursor as described in Example 2A) in methanolether at 0°C is treated with 6α-fluoro-11β,16α,17,21-tetrahydroxypregna-1,4-diene-3,20-dione, 16,17-cycloborate until nitrogen evolution ceases. The solution is evaporated to give the title compound.

WORKUP

后处理

  1. customThe solution is evaporated