HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12951531, compound → HCID 178426300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12951531 | HCID 12951531 | — |
| Reactant | HCID 178504065 | HCID 178504065 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178426300 | HCID 178426300 | — |
Reaction Steps
A solution of 3-methyl-2-((2-aminoethyl)thiomethyl)pyridine (6.3 g) and N-benzenesulphonyl-S-methylisothiourea (8.0 g) in acetonitrile (100 ml) was heated under reflux for 24 hours. Concentration, followed by chromatographic purification on a column of silica gel and recrystallisation afforded N-benzenesulphonyl-N'-[2-((3-methyl-2-pyridyl)methylthio)ethyl] guanidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03971786 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-d4ad78684e0445248c303b468e475b5a |
| Source note | uspto-grants-1976_07 |