HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 178464563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Ethyl 3-hydroxybenzo(b)thiophene-2-carboximidate | HCID 3040799 | — |
| Product | HCID 178464563 | HCID 178464563 | 67% |
Reaction Steps
3 g of ethyl 3-hydroxy-benzo[b]thiophene-2-carboximidate (Example 2) are heated under reflux for 10 hours in 20 g of 33% aqueous ethylamine solution. The residue obtained after evaporation is recrystallized from an ethyl acetate/isopropanol solution and yields 2 g of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03971814 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-7d6f3dc348fd4f9994226bf8ca7a731a |
| Source note | uspto-grants-1976_07 |