HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21521259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86733766 | HCID 86733766 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21521259 | HCID 21521259 | — |
Reaction Steps
22.5g (0.08 mol) of N-(2-benzoylmercaptopropionyl-β-alanine was added to the solution of 10.0g (0.25 mol) of NaOH in 100 ml of water to allow the β-alanine derivative to hydrolyze at 40°C for 1 hour. The reaction mixture was acidified with hydrochloric acid and, after distilling off the benzoic acid, concentrated to give 8.8g of N-(2-mercaptopropionyl-βalanine, ##EQU11##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03971828 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-708a2cf122c443a0ac5f07e0cafc199c |
| Source note | uspto-grants-1976_07 |