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HRID918611

反应详情

EQUATION

反应方程式

HRID 918611 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：Nc1ccccc1
HCID6115

Aniline

C6H7N

结构：NS(=O)(=O)c1cc(C(=O)O)cc([N+](=O)[O-])c1Cl
HCID89893

4-Chloro-3-nitro-5-sulphamoylbenzoic acid

C7H5ClN2O6S

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1cc(C(=O)O)cc([N+](=O)[O-])c1Nc1ccccc1
HCID21506071

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

CONDITIONS

反应条件

温度
80 °C

PROCEDURE

实验过程

A mixture of 4-chloro-3-nitro-5-sulphamyl-benzoic acid (8.4 g), aniline (8.4 g), and water (40 ml) was stirred at 80°C for 2 hours. After the addition of 1N hydrochloric acid (50 ml) and cooling, the precipitated 4-anilino-3-nitro-5-sulphamyl-benzoic acid was collected by suction, washed with water, and recrystallized from aqueous ethanol. The melting point was 261°-262°C.

WORKUP

后处理

  1. temperaturecooling
  2. customthe precipitated 4-anilino-3-nitro-5-sulphamyl-benzoic acid was collected by suction
  3. washwashed with water
  4. customrecrystallized from aqueous ethanol