HRID918670

反应详情

EQUATION

反应方程式

HRID 918670 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Ethyl-3-allylamino-4-phenoxy-5-sulphamyl-benzoate (1 g) was dissolved in 1N sodium hydroxide (15 ml) and left standing at room temperature for 24 hours. Then water (5 ml) was added, and the pH was adjusted to 3 by the addition of 4N hydrochloric acid. The precipitated 3-allylamino-4-phenoxy-5-sulphamyl-benzoic acid was collected and dried. The melting point was 223°-225°C.

WORKUP

后处理

  1. waitleft
  2. customThe precipitated 3-allylamino-4-phenoxy-5-sulphamyl-benzoic acid was collected
  3. customdried