HRID919087

反应详情

EQUATION

反应方程式

HRID 919087 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1-[4′-(5-tert-Butoxycarbonylamino-1-methyl-1H-pyrazol-4-yl)-biphenyl-4-yl]-cyclopropanecarboxylic acid ethyl ester (0.49 g, 1.1 mmol) was dissolved in HCl (4 N in dioxane, 3 mL) and stirred at room temperature for 30 minutes. The reaction was concentrated to dryness to yield the title compound as the hydrochloride salt.

WORKUP

后处理

  1. concentrationThe reaction was concentrated to dryness