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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 919115Generated: October 31, 2026

Cyclohexanecarboxylic acid → Cyclohexanecarbonyl chloride

https://huagongshe.com/reaction/919115

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCyclohexanecarboxylic acidHCID 7413—
ReactantThionyl ChlorideHCID 24386—
ProductCyclohexanecarbonyl chlorideHCID 75938—

Reaction Conditions

Temperature30 °C

Reaction Steps

The mixture of cyclohexylcarboxylic acid (40 g) and SOCl2 (60 mL) was heated at 30° C. for 30 min and then at 50° C. for 3-5 hrs. The volatile materials were removed in vacuum and the residue was used for the next reaction without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09273005B2
Source datasetuspto-grants-2016_03
ORD IDord-d600726b417f4254a73fe3ec0f5f232c
Source noteuspto-grants-2016_03