HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-amino-5-bromo-N-(pyridin-4-yl)nicotinamide → 2-Amino-5-(2-tert-butylsulfamoyl-phenyl)-N-pyridin-4-yl-nicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-amino-5-bromo-N-(pyridin-4-yl)nicotinamide | HCID 62155416 | — |
| Reactant | 2-Tert.-butyl-sulfamoyl-benzeneboronic acid | HCID 67451655 | — |
| Product | 2-Amino-5-(2-tert-butylsulfamoyl-phenyl)-N-pyridin-4-yl-nicotinamide | HCID 71060960 | — |
Reaction Steps
Reaction of 2-amino-5-bromo-N-pyridin-4-yl-nicotinamide with 2-tert.-butyl-sulfamoyl-benzeneboronic acid gives “A64”; method 1: HPLC/MS: 1.41 min, [M+H]=426;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09273029B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-a873e04690ec4a6e9182de046575712f |
| Source note | uspto-grants-2016_03 |