HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(2-Methoxyethyl)amine → 2-Amino-5-{4-[bis-(2-methoxy-ethyl)-carbamoyl]-phenyl}-N-pyridin-4-yl-nicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(2-Methoxyethyl)amine | HCID 2383 | — |
| Reactant | 4-[6-Amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid | HCID 71061416 | — |
| Product | 2-Amino-5-{4-[bis-(2-methoxy-ethyl)-carbamoyl]-phenyl}-N-pyridin-4-yl-nicotinamide | HCID 71061516 | — |
Reaction Steps
Reaction of 4-[6-amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid with bis-(2-methoxy-ethyl)-amine gives “A89”; method 1: HPLC/MS: 1.30 min, [M+H]=450;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09273029B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-3b3f1013b2514b29914131c892e3c375 |
| Source note | uspto-grants-2016_03 |