Diethanolamine → HCID 71061213, compound

HRID 919270Notes

Reaction equation

HRID 919270 reaction equation
[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][C:11]([C:12]([OH:14])=O)=[CH:10][CH:9]=2)=[CH:4][C:3]=1[C:17](=[O:25])[NH:18][C:19]1[CH:24]=[CH:23][N:22]=[CH:21][CH:20]=1.[OH:26][CH2:27][CH2:28][NH:29][CH2:30][CH2:31][OH:32]>>[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[CH:10][C:11]([C:12](=[O:14])[N:29]([CH2:30][CH2:31][OH:32])[CH2:28][CH2:27][OH:26])=[CH:15][CH:16]=2)=[CH:4][C:3]=1[C:17]([NH:18][C:19]1[CH:20]=[CH:21][N:22]=[CH:23][CH:24]=1)=[O:25]

Participants

3

Reactant 2

HCID 8113DiethanolamineHCID 71061416HCID 71061416, compound

Product 1

HCID 71061213HCID 71061213, compound

Procedure

Reaction of 4-[6-amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid with 2-(2-hydroxy-ethylamino)-ethanol gives “A93”; method 2: HPLC/MS: 1.62 min, [M+H]=422;

Workup

  1. customgives “A93”
  2. custom1.62 min, [M+H]=422

Sources & evidence

ORD record
ord-d58e7e6d10344a839b8960103124394b
Source dataset
uspto-grants-2016_03
Patent number
US09273029B2

Reaction notes

Loading…