Diethylamine → HCID 71061028, compound

HRID 919275Notes

Reaction equation

HRID 919275 reaction equation
[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:9]=[C:10]([CH:14]=[CH:15][CH:16]=2)[C:11](O)=[O:12])=[CH:4][C:3]=1[C:17](=[O:25])[NH:18][C:19]1[CH:24]=[CH:23][N:22]=[CH:21][CH:20]=1.[CH2:26]([NH:28][CH2:29][CH3:30])[CH3:27]>>[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][CH:14]=[C:10]([C:11](=[O:12])[N:28]([CH2:29][CH3:30])[CH2:26][CH3:27])[CH:9]=2)=[CH:4][C:3]=1[C:17]([NH:18][C:19]1[CH:20]=[CH:21][N:22]=[CH:23][CH:24]=1)=[O:25]

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 710607733-[6-Amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid

Product 1

HCID 71061028HCID 71061028, compound

Procedure

Reaction of 3-[6-amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid with diethyl amine gives “A98”; method 1: HPLC/MS: 1.37 min, [M+H]=390;

Workup

  1. customgives “A98”
  2. custom1.37 min, [M+H]=390

Sources & evidence

ORD record
ord-5c898fbd97a140a4aec0805d036d9251
Source dataset
uspto-grants-2016_03
Patent number
US09273029B2

Reaction notes

Loading…