Diethylamine → HCID 71061590, compound

HRID 919277Notes

Reaction equation

HRID 919277 reaction equation
[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][CH:14]=[CH:13][C:9]=2[C:10]([OH:12])=O)=[CH:4][C:3]=1[C:17](=[O:25])[NH:18][C:19]1[CH:24]=[CH:23][N:22]=[CH:21][CH:20]=1.[CH2:26]([NH:28][CH2:29][CH3:30])[CH3:27]>>[NH2:1][C:2]1[N:7]=[CH:6][C:5]([C:8]2[CH:16]=[CH:15][CH:14]=[CH:13][C:9]=2[C:10](=[O:12])[N:28]([CH2:29][CH3:30])[CH2:26][CH3:27])=[CH:4][C:3]=1[C:17]([NH:18][C:19]1[CH:20]=[CH:21][N:22]=[CH:23][CH:24]=1)=[O:25]

Participants

3

Reactant 2

HCID 8021DiethylamineHCID 71060940HCID 71060940, compound

Product 1

HCID 71061590HCID 71061590, compound

Procedure

Reaction of 2-[6-amino-5-(pyridin-4-ylcarbamoyl)-pyridin-3-yl]-benzoic acid with diethyl amine gives “A100”; method 2: HPLC/MS: 1.35 min, [M+H]=390;

Workup

  1. customgives “A100”
  2. custom1.35 min, [M+H]=390

Sources & evidence

ORD record
ord-e4d72ea41d86409890fe991bffe63eb4
Source dataset
uspto-grants-2016_03
Patent number
US09273029B2

Reaction notes

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