Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 919372Generated: October 31, 2026

HCID 117653658, compound → HCID 90421591, compound

https://huagongshe.com/reaction/919372

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 117653658HCID 117653658—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 90421591HCID 90421591114.4%

Reaction Steps

520 mg (1.45 mmol) of benzyl 1′-(oxetan-3-yl)-[4,4′-bipiperidine]-1-carboxylate was dissolved in 30 ml methanol and hydrogenated in the H-cube® flow hydrogenator using a 10 mol % Pd (C) cartridge at a flow rate of 1 ml/min. The solvent was removed in vacuo providing 372 mg of the title compound which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09273036B2
Source datasetuspto-grants-2016_03
ORD IDord-e9d517f436d44504ba4b6ce5cc57b52a
Source noteuspto-grants-2016_03