HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 117653658, compound → HCID 90421591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 117653658 | HCID 117653658 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 90421591 | HCID 90421591 | 114.4% |
Reaction Steps
520 mg (1.45 mmol) of benzyl 1′-(oxetan-3-yl)-[4,4′-bipiperidine]-1-carboxylate was dissolved in 30 ml methanol and hydrogenated in the H-cube® flow hydrogenator using a 10 mol % Pd (C) cartridge at a flow rate of 1 ml/min. The solvent was removed in vacuo providing 372 mg of the title compound which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09273036B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-e9d517f436d44504ba4b6ce5cc57b52a |
| Source note | uspto-grants-2016_03 |