HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 89533772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 117635545 | HCID 117635545 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 89533772 | HCID 89533772 | — |
Reaction Steps
In a 10 dram vial, added 7-1 (292.5 mg, 0.958 mmol) to DCM (3831 μl) and TFA (958 μl). After 30 min at RT, concentrated to give a clear, colorless oil. Carried crude material forward to subsequent step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09273040B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-f1a2604c83ff48758d8aee135ee67694 |
| Source note | uspto-grants-2016_03 |