HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86680251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 99710-75-5 | HCID 4115076 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86680251 | HCID 86680251 | — |
Reaction Steps
Preparation in accordance with Organikum [Practical Organic Chemistry], VEB Deutscher Verlag der Wissenschaften, Berlin, 5th Edition, 1965, page 409, by boiling 3,5-bisphenylbenzoic acid [99710-75-5] with 2 equivalents of thionyl chloride with addition of 2 drops of DMF. Yield: quantitative. Purity: >98% according to 1H-NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09273080B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-ab5cc7def04b41a69275591904d3fe4e |
| Source note | uspto-grants-2016_03 |