HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 86668819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Tricyclo(3.3.1.13,7)dec-1-ylmethylamine | HCID 86625 | — |
| Reactant | HCID 86668818 | HCID 86668818 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86668819 | HCID 86668819 | — |
Reaction Steps
To a solution of 4,6-dichloro-N-[4-(dimethylphosphoryl)phenyl]-1,3,5-triazin-2-amine (0.072 mmol) in 1.5 mL of ethanol is added 10 L of triethylamine and 1-(1-adamantyl)-methanamine (7.2 mg, 0.072 mmol). The mixture can be microwaved at 120 degrees for 20 minutes. The reaction mixture is filtered through a syringe filter and purified by prep-HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09273077B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-6c4a84ecc67f4138a5bf984546c6e0b8 |
| Source note | uspto-grants-2016_03 |