huagongshe.com
HRID921513

反应详情

EQUATION

反应方程式

HRID 921513 的结构方程式

REACTANTS

反应物

2
结构：CC(C)[SiH](C(C)C)C(C)C
HCID138754

Tri(propan-2-yl)silane

C9H22Si

结构：CC(C)(C)OC(=O)NCCC[P+](c1ccccc1)(c1ccccc1)c1ccccc1.[Br-]
HCID86685025

未命名化合物

PRODUCTS

生成物

1
结构：[Br-].[Br-].[NH3+]CCC[P+](c1ccccc1)(c1ccccc1)c1ccccc1
HCID178419277

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl.O=C(O)C(F)(F)F
溶剂HCID21863450

未命名化合物

PROCEDURE

实验过程

The solution of TFA/CH2Cl2 (1:1, 50 ml) containing triisoproylsilane (0.2 ml) was added to (3-((tert-butoxycarbonyl)amino) propyl)triphenylphosphonium bromide (6.15 g, 14.6 mmol). The mixture was stirred for 2 hours. After removal of the solvent, the compound was dried over vacuum and directly used in next step.

WORKUP

后处理

  1. customAfter removal of the solvent
  2. customthe compound was dried over vacuum