HuagongsheHuagongshe Chemistry Print Report · For research reference only
Silane, tris(1-methylethyl)- → HCID 178419277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Silane, tris(1-methylethyl)- | HCID 138754 | — |
| Reactant | HCID 86685025 | HCID 86685025 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 178419277 | HCID 178419277 | — |
Reaction Steps
The solution of TFA/CH2Cl2 (1:1, 50 ml) containing triisoproylsilane (0.2 ml) was added to (3-((tert-butoxycarbonyl)amino) propyl)triphenylphosphonium bromide (6.15 g, 14.6 mmol). The mixture was stirred for 2 hours. After removal of the solvent, the compound was dried over vacuum and directly used in next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09273343B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-61893a2533b445968313a839c50402eb |
| Source note | uspto-grants-2016_03 |