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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 921976Generated: October 25, 2026

Dimethyloctadecylamine → Triethoxysilylpropyl steardimonium chloride

https://huagongshe.com/reaction/921976

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyloctadecylamineHCID 15365—
Reactant(3-Chloropropyl)triethoxysilaneHCID 78771—
SolventEthanolHCID 702—
ProductTriethoxysilylpropyl steardimonium chlorideHCID 9807252150.4%

Reaction Conditions

Temperature135 °C

Reaction Steps

Firstly, 41.5 g (0.17 moL) of triethoxysilylpropyl chloride (Tokyo Kasei Kogyo Co., Ltd.), 44.6 g (0.150 moL) of N,N-dimethyl octadecylamine (Tokyo Kasei Kogyo Co., Ltd.) and 40.5 g of ethanol are fed into a nitrogen-purged pressurized reactor and heated to 135° C. After the reaction for 20 hours, 121.4 g of dimethyloctadecyl[3-(triethoxysilyl)propyl]ammonium chloride (EtAC) in ethanol solution is obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09278107B2
Source datasetuspto-grants-2016_03
ORD IDord-5bceff8534ce4e3e8af18bec98044369
Source noteuspto-grants-2016_03