Salicylic Acid → HCID 66764233, compound

HRID 921988Notes

Reaction equation

HRID 921988 reaction equation
[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[OH-].O[CH2:13][CH2:14][N+:15]([CH3:18])([CH3:17])[CH3:16]>CO>[C:1]([O:10][CH2:13][CH2:14][N+:15]([CH3:18])([CH3:17])[CH3:16])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4]

Participants

4

Reactant 2

HCID 338Salicylic AcidHCID 31255Choline, hydroxide

Product 1

HCID 66764233HCID 66764233, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Salicylic acid (5 or 10 mmol) and choline hydroxide (5 mmol, 40% solution in MeOH) were dissolved in 20 ml of methanol and stirred for 15 min at room temperature. The solvent was evaporated and the remaining viscous liquid was dried at 0.1 mbar with stirring for 24 hrs.

Workup

  1. customThe solvent was evaporated
  2. customthe remaining viscous liquid was dried at 0.1 mbar
  3. stirringwith stirring for 24 hrs

Sources & evidence

ORD record
ord-159a618c19cf45c1aedf692a69afad67
Source dataset
uspto-grants-2016_03
Patent number
US09278134B2

Reaction notes

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