Salicylic Acid → HCID 178443019, compound

HRID 921989Notes

Reaction equation

HRID 921989 reaction equation
[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:11]([O-:20])(=[O:19])[C:12]1[C:13](=[CH:15][CH:16]=[CH:17][CH:18]=1)[OH:14].[CH2:21]([N+:37]1[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=1)[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]>CC(C)=O>[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[CH2:21]([N+:37]1[CH:38]=[CH:39][CH:40]=[CH:41][CH:42]=1)[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36].[C:11]([OH:20])(=[O:19])[C:12]1[C:13](=[CH:15][CH:16]=[CH:17][CH:18]=1)[OH:14]

Participants

4

Reactant 2

HCID 338Salicylic AcidHCID 178443018HCID 178443018, compound

Product 1

HCID 178443019HCID 178443019, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

Salicylic acid (5-15 mmol) and cetylpyridinium salicylate (5 mmol) were dissolved in 20 ml of acetone and stirred for 15 min at room temperature. The solvent was evaporated and the remaining viscous liquid was dried at 0.1 mbar with stirring for 24 hrs.

Workup

  1. customThe solvent was evaporated
  2. customthe remaining viscous liquid was dried at 0.1 mbar
  3. stirringwith stirring for 24 hrs

Sources & evidence

ORD record
ord-063974fcfc2b46e7b5d5aa98b01f41ba
Source dataset
uspto-grants-2016_03
Patent number
US09278134B2

Reaction notes

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