HRID921989

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID338

Salicylic acid

C7H6O3

结构：CCCCCCCCCCCCCCCC[n+]1ccccc1.O=C([O-])c1ccccc1O

HCID178443018

未命名化合物

PRODUCTS

生成物

结构：CCCCCCCCCCCCCCCC[n+]1ccccc1.O=C(O)c1ccccc1O.O=C([O-])c1ccccc1O

HCID178443019

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

Salicylic acid (5-15 mmol) and cetylpyridinium salicylate (5 mmol) were dissolved in 20 ml of acetone and stirred for 15 min at room temperature. The solvent was evaporated and the remaining viscous liquid was dried at 0.1 mbar with stirring for 24 hrs.

WORKUP

后处理

customThe solvent was evaporated
customthe remaining viscous liquid was dried at 0.1 mbar
stirringwith stirring for 24 hrs

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-063974fcfc2b46e7b5d5aa98b01f41ba
来源数据集: uspto-grants-2016_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US09278134B2
来源说明: uspto-grants-2016_03

反应 SMILES

[C:1]([OH:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[C:11]([O-:20])(=[O:19])[C:12]1[C:13](=[CH:15][CH:16]=[CH:17][CH:18]=1)[OH:14].[CH2:21]([N+:37]1[CH:42]=[CH:41][CH:40]=[CH:39][CH:38]=1)[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36]>CC(C)=O>[C:1]([O-:10])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[OH:4].[CH2:21]([N+:37]1[CH:38]=[CH:39][CH:40]=[CH:41][CH:42]=1)[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH3:36].[C:11]([OH:20])(=[O:19])[C:12]1[C:13](=[CH:15][CH:16]=[CH:17][CH:18]=1)[OH:14]