反应详情

Cetylpyridinium salicylate (2 mmol) and clofibric acid (2 mmol) were grinded for 15 minutes in a mortar until a colourless cream was obtained. Identity and purity of the obtained product was confirmed via 1H NMR. 1H-NMR (300 MHz, d6-DMSO) δ(ppm)=9.13 (d, J=6.3 Hz, 2H), 8.60 (t, J=7.7 Hz, 1H), 8.16 (t, J=7.0 Hz, 2H), 7.67 (d, 8.0 Hz, 1H), 7.28 (d, J=9.1 Hz, 2H), 7.14 (t, J=6.7, 1H), 6.84 ((d, J=9.1 Hz, 2H), 6.61 (m, 2H), 4.59 (t, J=7.5 Hz, 2H), 1.89 (m, 2H), 1.47 (s, 6H), 1.22 (s, 27H), 0.84 (t, J=7.0 Hz, 3H). mp 8° C., T5%onset 197° C.

1. customwas obtained
2. custommp 8° C., T5%onset 197° C.