HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66686186, compound → HCID 88581364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66686186 | HCID 66686186 | — |
| Reactant | (4-{[(2E)-2-(methoxyimino)-2-phenylethyl]oxy}phenyl)methanol | HCID 86695770 | — |
| Product | HCID 88581364 | HCID 88581364 | 57.47% |
Reaction Steps
Compound 59 was synthesized from (1Z)-2-[4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime (2.34 g, 8.66 mmol) and ethyl 3-cyano-3-(4-hydroxyphenyl)butanoate (2.4 g, 9.6 mmol) by following the procedure described in scheme 18 (0.15 g, yield: 57.47%); Purity: 98.34%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278915B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-c9e9a6ff07714dc9be8be06676b30903 |
| Source note | uspto-grants-2016_03 |