HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66686187, compound → HCID 87111511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66686187 | HCID 66686187 | — |
| Reactant | (4-{[(2E)-2-(methoxyimino)-2-phenylethyl]oxy}phenyl)methanol | HCID 86695770 | — |
| Product | HCID 87111511 | HCID 87111511 | 95.69% |
Reaction Steps
Compound 62 was synthesized from (1Z)-2-[4-(hydroxymethyl)phenoxy]-1-phenylethanone O-methyloxime (0.5 g, 1.85 mmol) and methyl 3-cyano-3-(4-hydroxy-2-methylphenyl)propanoate (0.404 g, 1.85 mmol) by following the procedure described in scheme 18 (0.65 g, yield: 95.69%); Purity: 93.64%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278915B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-73e2ee221a644a4e8c6870b0060f669f |
| Source note | uspto-grants-2016_03 |