HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 56640644, compound → HCID 56640713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 56640644 | HCID 56640644 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 56640713 | HCID 56640713 | 36% |
Reaction Steps
Compound 96 was synthesized from ethyl 3-{2-(cyanomethoxy)-4-[(4-{[(2Z)-2-(methoxyimino)-2-phenylethyl]oxy}benzyl)oxy]phenyl}propanoate (Intermediate 134, 0.1 g, 0.199 mmol) and Pd—C (0.02 g), followed by hydrolysis described in scheme 16 (0.005 g, yield: 36.0%); Purity: 93.97%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278915B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-a892c38b73c440a68006d3a9096bc7c7 |
| Source note | uspto-grants-2016_03 |