6-Methoxypyridine-3-carbaldehyde → HCID 178519721, compound

Participants

Reaction Conditions

Reaction Steps

To A 100 mL RB was charged with 6-methoxypyridine-3-carbaldehyde (1 g, 7 mmol) was added 3N HCl (20 mL) and then refluxed it at 100° C. for 12 h. RM was cooled slowly to RT. Solid was obtained up on cooling. It was filtered off on Buchner flask and dried under line vacuum to obtain the title compound as white crystals (0.3 g, Yield: 37%)

Provenance & Evidence