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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 922305Generated: October 30, 2026

HCID 86695786, compound → HCID 66685529, compound

https://huagongshe.com/reaction/922305

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86695786HCID 86695786—
CatalystHCID 178418390HCID 178418390—
SolventEthanol ethylacetateHCID 21584252—
ProductHCID 66685529HCID 6668552995%

Reaction Steps

A solution of ethyl (2E)-3-(6-{[4-(2-oxo-2-phenylethoxy)benzyl]oxy}pyridin-3-yl)prop-2-enoate (0.13 g, 0.31 mmol) in ethyl acetate ethanol mixture was degassed well and added palladium carbon (10 mg), and stirred under hydrogen bladder for 3 hrs. Reaction mass was filtered through celite pad and concentrated to a colourless oil (0.12 g, Yield: 95%); MS (ESI, 120 eV): m/z=420 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09278915B2
Source datasetuspto-grants-2016_03
ORD IDord-fa598382560249a3853549ce346e4f62
Source noteuspto-grants-2016_03