HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86695786, compound → HCID 66685529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86695786 | HCID 86695786 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol ethylacetate | HCID 21584252 | — |
| Product | HCID 66685529 | HCID 66685529 | 95% |
Reaction Steps
A solution of ethyl (2E)-3-(6-{[4-(2-oxo-2-phenylethoxy)benzyl]oxy}pyridin-3-yl)prop-2-enoate (0.13 g, 0.31 mmol) in ethyl acetate ethanol mixture was degassed well and added palladium carbon (10 mg), and stirred under hydrogen bladder for 3 hrs. Reaction mass was filtered through celite pad and concentrated to a colourless oil (0.12 g, Yield: 95%); MS (ESI, 120 eV): m/z=420 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278915B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-fa598382560249a3853549ce346e4f62 |
| Source note | uspto-grants-2016_03 |