HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 20213340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 86695790 | HCID 86695790 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20213340 | HCID 20213340 | 71.4% |
Reaction Steps
To a solution of ethyl (2E)-3-(4′-methoxybiphenyl-4-yl)prop-2-enoate (1 g, 3.5 mmol) in ethyl acetate was added acetic acid and degassed well with argon and added palladium carbon (100 mg) and stirred under hydrogen for overnight, TLC shows a new spot, RM filtered through celite and washed with ethyl acetate and concentrated to afford white solid (0.7 g, Yield: 71.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278915B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-bfd2c430dc6540d3a2476094ca817fe8 |
| Source note | uspto-grants-2016_03 |