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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 922310Generated: November 1, 2026

Acetic Acid → HCID 20213340, compound

https://huagongshe.com/reaction/922310

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AcidHCID 176—
ReactantHCID 86695790HCID 86695790—
SolventEthyl AcetateHCID 8857—
ProductHCID 20213340HCID 2021334071.4%

Reaction Steps

To a solution of ethyl (2E)-3-(4′-methoxybiphenyl-4-yl)prop-2-enoate (1 g, 3.5 mmol) in ethyl acetate was added acetic acid and degassed well with argon and added palladium carbon (100 mg) and stirred under hydrogen for overnight, TLC shows a new spot, RM filtered through celite and washed with ethyl acetate and concentrated to afford white solid (0.7 g, Yield: 71.4%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09278915B2
Source datasetuspto-grants-2016_03
ORD IDord-bfd2c430dc6540d3a2476094ca817fe8
Source noteuspto-grants-2016_03